HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 136340738, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | HCID 136138660 | HCID 136138660 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 136340738 | HCID 136340738 | — |
Reaction Steps
A mixture of 13.0 g (29.6 mmol) of 2,4-diphenyl-6-(2'-hydroxy4'-(2"-hydroxycyclohexyloxy)phenyl)-1,3,5-triazine, 7.0 g (89.2 mmol) of acetyl chloride (Fluka, 99%) and 0.6 g (7.6 mmol) of pyridine in 140 ml of toluene (Merck, 99.5%) is stirred under nitrogen and held at 50° C. for 6 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05959008 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-3db426fa9cdf44c697aae59cc00794c4 |
| Source note | uspto-grants-1999_09 |