Potassium Carbonate → HCID 21846980, compound

Participants

Reaction Conditions

Reaction Steps

According to the method in Example 10, a mixture of 5-isoquinolinethiol 1.12 g (6.9 mmol), DMF 20 ml, potassium carbonate 1.92 g (13.9 mmol) and 2-chloro-5-nitropyridine 1.00 g (6.3 mmol) was stirred at 100° C. for 2 hours, and 5-[(5-nitro-2-pyridyl)-sulfanyl)isoquinoline 1.40 g (78.4%) was obtained.

Provenance & Evidence