HuagongsheHuagongshe Chemistry Print Report · For research reference only
(E)-2-phenylethene-1-sulfonyl chloride → HCID 53737535, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (E)-2-phenylethene-1-sulfonyl chloride | HCID 5369377 | — |
| Reactant | 3-(3-(S)-Amino-2-oxopyrrolidin-1-ylmethyl)benzonitrile hydrochloride | HCID 22870786 | — |
| Product | HCID 53737535 | HCID 53737535 | — |
Reaction Steps
The title compound is prepared from 3-(3-(S)-amino-2-oxopyrrolidin-1-ylmethyl)benzonitrile hydrochloride as in EXAMPLE 24, Part B using trans-b-styrenesulfonyl chloride in place of 6-methoxynaphthalene-2-sulfonyl chloride. The crude product is triturated from 50% EtOAc/hexanes to give the title compound as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05958918 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-e00e6d64aeb64fa08fbda3f650e43550 |
| Source note | uspto-grants-1999_09 |