HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl iodide → HCID 67365974, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl iodide | HCID 12098 | — |
| Reactant | HCID 54497438 | HCID 54497438 | — |
| Product | HCID 67365974 | HCID 67365974 | — |
Reaction Steps
The title compound is prepared as described in EXAMPLE 25, Part A using 4,5-dichlorothiophene-2-sulfonic acid [1-(3-cyanobenzyl)-2-oxopyrrolidin-3-(S)-yl]amide, prepared as described in EXAMPLE 80, part A, and benzyl iodide. The crude product is purified by column chromatography eluting with gradient of 20% EtOAc/hexanes to 40% EtOAc/hexanes to afford the title compound as a white foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05958918 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-ed917609fba549329c709304745b3410 |
| Source note | uspto-grants-1999_09 |