HuagongsheHuagongshe Chemistry Print Report · For research reference only
7-methoxynaphtalene-2-sulfonic acid [1-(3-cyanobenzyl)-2-oxopyrrolidin-3-(S)-yl]amide → HCID 10768584, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 7-methoxynaphtalene-2-sulfonic acid [1-(3-cyanobenzyl)-2-oxopyrrolidin-3-(S)-yl]amide | HCID 10550854 | — |
| Reactant | 2-(Bromomethyl)thiophene | HCID 11829978 | — |
| Product | HCID 10768584 | HCID 10768584 | — |
Reaction Steps
The title compound is prepared as described in EXAMPLE 90, Part A using 7-methoxynaphthalene-2-sulfonic acid [1-(3-cyanobenzyl)-2-oxopyrrolidin-3-(S)-yl]amide (0.100 g, 0.23 mmol), prepared as described in EXAMPLE 43, part A, and thiophene-2-ylmethyl bromide (0.10 g, 0.56 mmol). The crude product is triturated with hexane/ether and used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05958918 |
| Source dataset | uspto-grants-1999_09 |
| ORD ID | ord-aa32c85161f1452e8c0c415f7a6c5327 |
| Source note | uspto-grants-1999_09 |