HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfamide → HCID 21247719, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfamide | HCID 82267 | — |
| Reactant | HCID 21247967 | HCID 21247967 | — |
| Solvent | Sulfolane | HCID 31347 | — |
| Product | HCID 21247719 | HCID 21247719 | — |
Reaction Steps
A solution of 29.5 g of p-(5-pentyl-2-tetrahydropyranyl)benzoyl chloride and 8 g of sulfamide in 500 ml of tetramethylene sulfone is heated at 120° for 4 hours, evaporated and worked up as usual. 2-p-cyanophenyl-5-pentyltetrahydropyran is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04818431 |
| Source dataset | uspto-grants-1989_04 |
| ORD ID | ord-5586723f6cf64843957c7580ea84c56b |
| Source note | uspto-grants-1989_04 |