HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 21247727, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-Iodohexane | HCID 12527 | — |
| Reactant | HCID 21247632 | HCID 21247632 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 21247727 | HCID 21247727 | — |
Reaction Steps
A mixture of 24.8 g of 2-p-hydroxyphenyl-5-pentyltetrahydropyran (obtainable by diazotization of 2-p-aminophenyl-5-pentyltetrahydropyran and hydrolysis), 6.9 g of K2CO3, 25 g of hexyl iodide and 250 ml of DMF is heated, with stirring, at 80° for 16 hours, then cooled and worked up as usual. 2-p-Hexoxyphenyl-5-pentyltetrahydropyran is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04818431 |
| Source dataset | uspto-grants-1989_04 |
| ORD ID | ord-fc6b8145074d4db989187d3ada88a079 |
| Source note | uspto-grants-1989_04 |