HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Dimethylamino)-1-phenylethanol → N,N-Dimethylphenylethylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Dimethylamino)-1-phenylethanol | HCID 120846 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | N,N-Dimethylphenylethylamine | HCID 25125 | — |
Reaction Steps
As Example 15 but using 2-dimethylamino-1-phenyl-ethanol (13.7 g) instead of 3-acetylpyridine. The crude material is pyrified by column chromatography on aluminium oxide using dichloromethane as eluant. The product is dried in vacuo to constant weight to give 1-(1,3-dithian-2-ylidene)-2-ylidene)-2-dimethylamino-1-phenylethane as an oil at room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04818765 |
| Source dataset | uspto-grants-1989_04 |
| ORD ID | ord-e0339d7105714941bca1842eb68379c8 |
| Source note | uspto-grants-1989_04 |