HCID 14324671, compound → 3-tert-butyl-4-methoxybenzaldehyde

HRID 620126Notes

Reaction equation

HRID 620126 reaction equation
C[O:2][CH:3](OC)[C:4]1[CH:9]=[CH:8][C:7]([O:10][CH3:11])=[C:6]([C:12]([CH3:15])([CH3:14])[CH3:13])[CH:5]=1>O>[C:12]([C:6]1[CH:5]=[C:4]([CH:9]=[CH:8][C:7]=1[O:10][CH3:11])[CH:3]=[O:2])([CH3:15])([CH3:13])[CH3:14]

Participants

3

Reactant 1

HCID 14324671HCID 14324671, compound

Product 1

HCID 37746043-tert-butyl-4-methoxybenzaldehydeYield 96.7%

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

99.4 g of 3-tert-butyl-4-methoxybenzaldehyde dimethyl acetal are refluxed in 300 g of water for 3 hours. This is followed by cooling down, and the residue is filtered off and dried, leaving 77.5 g of 3-tert-butyl-4-methoxybenzaldehyde (mp. 52°-53 C.), which corresponds to a yield of 96.7%.

Workup

  1. temperatureby cooling down
  2. filtrationthe residue is filtered off
  3. customdried

Sources & evidence

ORD record
ord-7936ff03a77a42bf915fae722d1761e7
Source dataset
uspto-grants-1989_04
Patent number
US04820389

Reaction notes

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