HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14324671, compound → 3-tert-butyl-4-methoxybenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14324671 | HCID 14324671 | — |
| Solvent | Water | HCID 962 | — |
| Product | 3-tert-butyl-4-methoxybenzaldehyde | HCID 3774604 | 96.7% |
Reaction Steps
99.4 g of 3-tert-butyl-4-methoxybenzaldehyde dimethyl acetal are refluxed in 300 g of water for 3 hours. This is followed by cooling down, and the residue is filtered off and dried, leaving 77.5 g of 3-tert-butyl-4-methoxybenzaldehyde (mp. 52°-53 C.), which corresponds to a yield of 96.7%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04820389 |
| Source dataset | uspto-grants-1989_04 |
| ORD ID | ord-7936ff03a77a42bf915fae722d1761e7 |
| Source note | uspto-grants-1989_04 |