HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formaldehyde → HCID 23044696, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | HCID 601065 | HCID 601065 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 23044696 | HCID 23044696 | 68.3% |
Reaction Steps
20.20 g (44.0 mmol) of tetra-n-pentyl methylenebisphosphonate, 6.61 g (220.0 mmol) of paraformaldehyde and 3.22 g (64.0 mmol) of diethylamine are combined with the same reactants and the same conditions as described above in Example I. This mixture is then refluxed for 48 hours. After the methanol is eliminated as described above in Example I. 14.08 g of tetra-n-pentyl ethenylidenebisphosphonate is produced as a clear liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04820698 |
| Source dataset | uspto-grants-1989_04 |
| ORD ID | ord-2694c32d22aa4e1db1baf50518b7bcb9 |
| Source note | uspto-grants-1989_04 |