HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyruvic Acid → HCID 70377797, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyruvic Acid | HCID 1060 | — |
| Reactant | HCID 18631782 | HCID 18631782 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 70377797 | HCID 70377797 | — |
Reaction Steps
To a solution of N-carbobenzoxy-L-valyl-N-benzyl glycine (17.2 g, 44.6 mmol) and pyruvic acid (19.6 g, 0.223 mol) in 400 ml absolute ethanol was added 10% palladium on carbon (1.5 g). The mixture was hydrogenated at 50 psi for 4 hours. Filtration and concentration in vacuo provided an oily product which was purified as in example 7D.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04820729 |
| Source dataset | uspto-grants-1989_04 |
| ORD ID | ord-274a43f332d4470cac594f8797b20b92 |
| Source note | uspto-grants-1989_04 |