HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66900711, compound → HCID 44241236, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66900711 | HCID 66900711 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 44241236 | HCID 44241236 | — |
Reaction Steps
A solution of tert-butyl[4-(4-amino-2-ethyl-1H-imidazo[4,5-c]quinolin-1-yl)butyl]tetrahydro-2H-pyran-4-ylcarbamate in trifluroacetic acid was stirred at 40° C. for 4 hrs. Reaction mixture was then poured on ice-water mixture and extracted with chloroform. Organic layer was dried over sodium sulphate and concentrated under deduced pressure to afford the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09446040B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-49367b0612614214825570693c4463a9 |
| Source note | uspto-grants-2016_09 |