Diethanolamine → HCID 14051962, compound

HRID 620443Notes

Reaction equation

HRID 620443 reaction equation
[CH3:1][O:2][CH2:3][CH2:4][NH:5][C:6]([C:8]1[N:12]([CH2:13][C:14](=[O:18])[NH:15]OC)[N:11]=[C:10]([N+:19]([O-:21])=[O:20])[N:9]=1)=[O:7].N(CCO)[CH2:23][CH2:24][OH:25].[O:29]1CCO[CH2:31][CH2:30]1>>[CH3:1][O:2][CH2:3][CH2:4][NH:5][C:6]([C:8]1[N:12]([CH2:13][C:14](=[O:18])[N:15]([CH2:31][CH2:30][OH:29])[CH2:23][CH2:24][OH:25])[N:11]=[C:10]([N+:19]([O-:21])=[O:20])[N:9]=1)=[O:7]

Participants

4

Reactant 3

HCID 8113DiethanolamineHCID 312751,4-DioxaneHCID 54018838HCID 54018838, compound

Product 1

HCID 14051962HCID 14051962, compound

Procedure

To 530 mg of 1-methoxycarbamoylmethyl-3-nitro-1,2,4-triazole-5-carboxylic acid methoxyethylamide dissolved in 3 ml of dioxane is added 1 g of diethanolamine.

Sources & evidence

ORD record
ord-86b4d946d1854cabae786f4206fa866a
Source dataset
uspto-grants-1989_04
Patent number
US04820844

Reaction notes

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