huagongshe.com
HRID620467

反应详情

EQUATION

反应方程式

HRID 620467 的结构方程式

REACTANTS

反应物

1
结构：CCCC(C)(COc1ccc([N+](=O)[O-])cc1)COc1ccc([N+](=O)[O-])cc1
HCID19860671

未命名化合物

PRODUCTS

生成物

1
结构：CCCC(C)(COc1ccc(N)cc1)COc1ccc(N)cc1
HCID19860674

Benzenamine, 4,4′-[(2-methyl-2-propyl-1,3-propanediyl)bis(oxy)]bis-

C19H26N2O2

AUXILIARIES

试剂、催化剂与溶剂

2
结构：[Ni]
催化剂HCID935

Nickel

Ni

结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

300 g 1,3-bis-(4-nitrophenoxy)-2-methyl-2-propylpropane were hydrogenated as in Example 10 in 1500 ml DMF in the presence of 46 g Raney nickel. The crude product was recrystallized from toluene.

WORKUP

后处理

  1. customThe crude product was recrystallized from toluene