HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15617525, compound → HCID 15617526, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15617525 | HCID 15617525 | — |
| Catalyst | Manganese oxide | HCID 160959 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 15617526 | HCID 15617526 | — |
Reaction Steps
To ethyl acetate (150 ml), cooled to 0° C., was added manganese oxide (15 g) followed by 2-(7-bromoheptyl) benzyl alcohol (3.39 g, 1.2 mmoles). The reaction mixture was permitted to warm to room temperature slowly, and stirred for 1 hour. The mixture was then cooled to 0° C. and stirred for 18 hours. Subsequently the mixture was filtered and evaporated to yield the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04820719 |
| Source dataset | uspto-grants-1989_04 |
| ORD ID | ord-6dafa169e2824cf2b11a15e793f8e521 |
| Source note | uspto-grants-1989_04 |