反应详情

A solution of 154 g (0.39 mol) of 2-(m-nitrophenoxy)-myristic acid ethyl ester in 500 ml of ethanol is placed in an autoclave. An amount of 8 ml of Raney nickel is added. Reduction of the nitro group is carried out with hydrogen gas at an initial pressure of 10-10.5 MPa and a temperature of 65° C. After the reduction (2 h) the solvent is removed by evaporation.

1. customa temperature of 65° C
2. customAfter the reduction (2 h) the solvent is removed by evaporation