HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 2-[m-(3-Chloro-2,2,3-trifluoro-propionamido)-phenoxy]-myristoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-[m-(3-Chloro-2,2,3-trifluoro-propionamido)-phenoxy]-myristic acid | HCID 14122418 | — |
| Product | 2-[m-(3-Chloro-2,2,3-trifluoro-propionamido)-phenoxy]-myristoyl chloride | HCID 14122419 | — |
Reaction Steps
An amount of 31.5 g of 2-[m-(3-chloro-2,2,3-trifluoro-propionamido)-phenoxy]-myristic acid is refluxed for 30 min with thionyl chloride. The excess thionyl chloride is removed by evaporation. The oil obtained slowly solidifies.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04822729 |
| Source dataset | uspto-grants-1989_04 |
| ORD ID | ord-c25c14b79c2447a1b79c6d206278d3dc |
| Source note | uspto-grants-1989_04 |