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HRID620703

反应详情

EQUATION

反应方程式

HRID 620703 的结构方程式

REACTANTS

反应物

2
结构：O=S(Cl)Cl
HCID24386

Thionyl chloride

Cl2OS

结构：CCCCCCCCCCCCC(Oc1ccc([N+](=O)[O-])cc1)C(=O)O
HCID3746500

2-(4-nitrophenoxy)-Tetradecanoic acid

C20H31NO5

PRODUCTS

生成物

1
结构：CCCCCCCCCCCCC(Oc1ccc([N+](=O)[O-])cc1)C(=O)Cl
HCID2735105

2-(4-nitrophenoxy)tetradecanoyl Chloride

C20H30ClNO4

PROCEDURE

实验过程

An amount of 550 g of 2-(p-nitrophenoxy)-myristic acid is heated together with 550 ml of thionyl chloride for 1 h to 60° C. so that a solution is obtained. The excess thionyl chloride is filtered off. Yield: 585 g (100%) of 2-(p-nitrophenoxyl]-myristoyl chloride (oil).

WORKUP

后处理

  1. customis obtained
  2. filtrationThe excess thionyl chloride is filtered off