HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 2-(4-nitrophenoxy)tetradecanoyl Chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-(4-nitrophenoxy)-Tetradecanoic acid | HCID 3746500 | — |
| Product | 2-(4-nitrophenoxy)tetradecanoyl Chloride | HCID 2735105 | — |
Reaction Steps
An amount of 550 g of 2-(p-nitrophenoxy)-myristic acid is heated together with 550 ml of thionyl chloride for 1 h to 60° C. so that a solution is obtained. The excess thionyl chloride is filtered off. Yield: 585 g (100%) of 2-(p-nitrophenoxyl]-myristoyl chloride (oil).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04822729 |
| Source dataset | uspto-grants-1989_04 |
| ORD ID | ord-88e05f05acff4e6bba31d87f86060279 |
| Source note | uspto-grants-1989_04 |