HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonyl chloride → 7-Methanesulphonamido-3-(6-methanesulphonamidoquinol-2-ylmethyl)-1,2,4,5-tetrahydro-3H-3-benzazepine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | 7-amino-3-(6-aminoquinol-2-ylmethyl)-1,2,4,5-tetrahydro-3H-3-benzazepine | HCID 21245054 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 7-Methanesulphonamido-3-(6-methanesulphonamidoquinol-2-ylmethyl)-1,2,4,5-tetrahydro-3H-3-benzazepine | HCID 21245057 | — |
Reaction Steps
The title compound, m.p. 207°-210°, was prepared similarly to the procedure of Example 1 starting from 7-amino-3-(6-aminoquinol-2-ylmethyl)-1,2,4,5-tetrahydro-3H-3-benzazepine and methanesulphonyl chloride in pyridine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04822793 |
| Source dataset | uspto-grants-1989_04 |
| ORD ID | ord-b6bb0e42d0e0426a828f660ac9eaa06e |
| Source note | uspto-grants-1989_04 |