Hydrochloric Acid → HCID 178488940, compound

HRID 620838Notes

Reaction equation

HRID 620838 reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[C:7]([O:9][CH3:10])[CH:6]=[CH:5][C:4]=1[C:11]1[NH:12][C:13]([C:17]2[CH:18]=[N:19][CH:20]=[CH:21][CH:22]=2)=[C:14]([CH3:16])[N:15]=1.[ClH:23]>C(O)C>[ClH:23].[ClH:23].[CH3:1][O:2][C:3]1[CH:8]=[C:7]([O:9][CH3:10])[CH:6]=[CH:5][C:4]=1[C:11]1[NH:12][C:13]([C:17]2[CH:18]=[N:19][CH:20]=[CH:21][CH:22]=2)=[C:14]([CH3:16])[N:15]=1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 178488939HCID 178488939, compound

Product 1

HCID 178488940HCID 178488940, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

To a solution of 2-(2,4-dimethoxyphenyl)-4-methyl-5-(3-pyridyl)imidazole (0.9 g) in ethanol (20 ml) was added conc. hydrochloric acid (0.6 ml), and the mixture was evaporated. The resulting syrup was triturated in ethanol to give 2-(2,4-dimethoxyphenyl)-4-methyl-5-(3-pyridyl)imidazole dihydrochloride (1.02 g).

Workup

  1. customthe mixture was evaporated
  2. customThe resulting syrup was triturated in ethanol

Sources & evidence

ORD record
ord-8fdfb5bfea264f7483d70136bc2177dd
Source dataset
uspto-grants-1989_04
Patent number
US04822805

Reaction notes

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