HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → 1-tert-Butyl-2,5-dichloro-4-methylbenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Product | 1-tert-Butyl-2,5-dichloro-4-methylbenzene | HCID 14418830 | 270.8% |
Reaction Steps
After adding a large excess of 2000 g of toluene and 64 g (0.48 mol) of anhydrous aluminum chloride, as a catalyst, to 284 g (1.3 mol) of 2,5-dichloro-4-t-butyltoluene obtained as stated above, the mixture was brought into reaction for 5 hours at room temperature under a vigorous agitation thereof.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04822928 |
| Source dataset | uspto-grants-1989_04 |
| ORD ID | ord-7d240177babf4591935d6a2ff34f315a |
| Source note | uspto-grants-1989_04 |