関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Cyromazine | HCID 47866 | — |
| 反応物 | Methoxyacetyl chloride | HCID 96623 | — |
| 溶媒 | Pyridine | HCID 1049 | — |
| 生成物 | HCID 21243170 | HCID 21243170 | — |
反応手順
7.2 g of methoxyacetyl chloride are slowly added dropwise to a suspension of 5.0 g of 2,4-diamino-6-cyclopropylamino-1,3,5-triazine in 50 ml of pyridine. The reaction mixture is subsequently stirred for 1 hour at 55° C. and then for 16 hours at room temperature. After filtration of the reaction mixture, washing of the filter residue with water and finally drying, the product is obtained as white crystalline powder having a melting point of 175°-180° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04824845 |
|---|
| 出典データセット | uspto-grants-1989_04 |
|---|
| ORD ID | ord-575bb544b3f7463cbafef8e1b91c713a |
|---|
| 出典メモ | uspto-grants-1989_04 |
|---|