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HRID 621427作成日:2026年10月25日

Cyromazine → HCID 21243170、化合物

https://huagongshe.com/reaction/621427

反応式

関与物質

役割名称HCID仕込み量
反応物CyromazineHCID 47866—
反応物Methoxyacetyl chlorideHCID 96623—
溶媒PyridineHCID 1049—
生成物HCID 21243170HCID 21243170—

反応条件

温度55 °C

反応手順

7.2 g of methoxyacetyl chloride are slowly added dropwise to a suspension of 5.0 g of 2,4-diamino-6-cyclopropylamino-1,3,5-triazine in 50 ml of pyridine. The reaction mixture is subsequently stirred for 1 hour at 55° C. and then for 16 hours at room temperature. After filtration of the reaction mixture, washing of the filter residue with water and finally drying, the product is obtained as white crystalline powder having a melting point of 175°-180° C.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04824845
出典データセットuspto-grants-1989_04
ORD IDord-575bb544b3f7463cbafef8e1b91c713a
出典メモuspto-grants-1989_04