huagongshe.com
HRID621435

反应详情

EQUATION

反应方程式

HRID 621435 的结构方程式

REACTANTS

反应物

2
结构：[NH4+].[OH-]
HCID14923

Ammonium hydroxide

H5NO

结构：COc1cc2c(cc1S(=O)(=O)Cl)CCN(C(C)=O)CC2
HCID13853350

未命名化合物

PRODUCTS

生成物

1
结构：COc1cc2c(cc1S(N)(=O)=O)CCN(C(C)=O)CC2
HCID13853351

未命名化合物

PROCEDURE

实验过程

3-Acetyl-7-chlorosulfonyl-8-methoxy-2,3,4,5-tetrahydro-1H-3-benzazepine (3 g, 0.007 m) was treated with concentrated ammonium hydroxide (10 ml), stirred for 2 hours and filtered to give 3-acetyl-8-methoxy-7-sulfamoyl-2,3,4,5-tetrahydro-1H-3-benzazepine, m.p. 260°-263°.

WORKUP

后处理

  1. filtrationfiltered