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HRID621441

反应详情

EQUATION

反应方程式

HRID 621441 的结构方程式

REACTANTS

反应物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：COc1cc2c(cc1S(C)(=O)=O)CCN(C(C)=O)CC2
HCID13853355

未命名化合物

PRODUCTS

生成物

1
结构：COc1cc2c(cc1S(C)(=O)=O)CCNCC2.Cl
HCID21242875

未命名化合物

PROCEDURE

实验过程

Alternatively, 3-acetyl-8-methoxy-7-methylsulfonyl-2,3,4,5-tetrahydro-1H-3-benzazepine was treated with 3N hydrochloric acid to give 8-methoxy-7-methylsulfonyl-2,3,4,5-tetrahydro-1H-3-benzazepine hydrochloride, m.p. 228.5°-229.5°. Refluxing this compound with 48% hydrobromic acid gave 8-hydroxy-7-methylsulfonyl-2,3,4,5-tetrahydro-1H-3-benzazepine hydrobromide.