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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 621459Generated: November 1, 2026

Hydrochloric Acid → HCID 21242901, compound

https://huagongshe.com/reaction/621459

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
Reactant3-acetyl-2,3,4,5-tetrahydro-1H-3-benzazepine-7-sulfonyl chlorideHCID 11346737—
ReactantHCID 21242874HCID 21242874—
ReactantHCID 21242882HCID 21242882—
ProductHCID 21242901HCID 21242901—

Reaction Steps

Following the procedure of Examples 4 and 5, 3-acetyl-7-chlorosulfonyl-2,3,4,5-tetrahydro-1H-3-benzazepine is converted to 3-acetyl-7-methylthio-2,3,4,5-tetrahydro-1H-3-benzazepine and then to 3-acetyl-7-methylsulfinyl-2,3,4,5-tetrahydro-1H-3-benzazepine which is hydrolyzed with dilute hydrochloric acid to give 7-methylsulfinyl-2,3,4,5-tetrahydro-1H-3-benzazepine hydrochloride.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04824839
Source datasetuspto-grants-1989_04
ORD IDord-20a6adb0b0ed4db3a4ef1b5258abd4fd
Source noteuspto-grants-1989_04