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HRID621459

反应详情

EQUATION

反应方程式

HRID 621459 的结构方程式

REACTANTS

反应物

4
反应SMILES：Cl
HCID313

Hydrochloric Acid

ClH

反应SMILES：CC(=O)N1CCc2ccc(S(=O)(=O)Cl)cc2CC1
HCID11346737

3-acetyl-7-chlorosulfonyl-2,3,4,5 -tetrahydro-1H-3-benzazepine

C12H14ClNO3S

反应SMILES：CSc1ccc2c(c1)CCN(C(C)=O)CC2
HCID21242874

未命名化合物

反应SMILES：CC(=O)N1CCc2ccc(S(C)=O)cc2CC1
HCID21242882

未命名化合物

PRODUCTS

产物

1
反应SMILES：CS(=O)c1ccc2c(c1)CCNCC2.Cl
HCID21242901

未命名化合物

PROCEDURE

实验过程

Following the procedure of Examples 4 and 5, 3-acetyl-7-chlorosulfonyl-2,3,4,5-tetrahydro-1H-3-benzazepine is converted to 3-acetyl-7-methylthio-2,3,4,5-tetrahydro-1H-3-benzazepine and then to 3-acetyl-7-methylsulfinyl-2,3,4,5-tetrahydro-1H-3-benzazepine which is hydrolyzed with dilute hydrochloric acid to give 7-methylsulfinyl-2,3,4,5-tetrahydro-1H-3-benzazepine hydrochloride.