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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 621474Generated: November 1, 2026

Methyl iodide → HCID 14100188, compound

https://huagongshe.com/reaction/621474

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl iodideHCID 6328—
ReactantPotassium CarbonateHCID 11430—
ReactantHCID 14100187HCID 14100187—
SolventDimethylformamideHCID 6228—
ProductHCID 14100188HCID 14100188—

Reaction Conditions

Temperature60 °C

Reaction Steps

A mixture of 5-ethyl-3-methylamino-7-(4-methylbenzyl)-2H-pyrazolo[3,4-d]pyrimidine-4,6(5H,7H)-dione (0.5 g, 1.6 mM), methyl iodide (0,46 g, 3.2 mM) and potassium carbonate (0,45 g, 3.2 mM) in DMF (8 ml) was stirred at 60° C. for 30 hours.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04824848
Source datasetuspto-grants-1989_04
ORD IDord-71ef4ce2e3d14b1b81daa88a1e4568bb
Source noteuspto-grants-1989_04