Morpholine → HCID 21243367, compound

HRID 621605Notes

Reaction equation

HRID 621605 reaction equation
[F:1][C:2]([F:8])([F:7])[S:3]([NH2:6])(=[O:5])=[O:4].[NH:9]1[CH2:14][CH2:13][O:12][CH2:11][CH2:10]1>CC(C)=O>[F:1][C:2]([F:8])([F:7])[S:3]([NH2:6])(=[O:5])=[O:4].[NH2+:9]1[CH2:14][CH2:13][O:12][CH2:11][CH2:10]1

Participants

4

Reactant 2

HCID 8083MorpholineHCID 79001Trifluoromethylsulfonamide

Product 1

HCID 21243367HCID 21243367, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

Trifluoromethanesulfonamide (14.9g, 0.10 mole), morpholine (8.7g, 0.10 mole) and acetone (100 ml) were stirred together for one hour. The solvent was evaporated in vacuo to give morpholinium trifluoromethanesulfonamide, m.p. 84°-87° C. Analysis: Calculated for C5H11F3N2O3S: %C 25.4; %H, 4.7; %N, 11.8; found: %C, 25.3;D %H, 4.7; %N, 11.7.

Workup

  1. customThe solvent was evaporated in vacuo

Sources & evidence

ORD record
ord-3fe8fea3431d49788cec5587b5bf1f83
Source dataset
uspto-grants-1989_04
Patent number
US04824866

Reaction notes

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