HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 21243367, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | Trifluoromethylsulfonamide | HCID 79001 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 21243367 | HCID 21243367 | — |
Reaction Steps
Trifluoromethanesulfonamide (14.9g, 0.10 mole), morpholine (8.7g, 0.10 mole) and acetone (100 ml) were stirred together for one hour. The solvent was evaporated in vacuo to give morpholinium trifluoromethanesulfonamide, m.p. 84°-87° C. Analysis: Calculated for C5H11F3N2O3S: %C 25.4; %H, 4.7; %N, 11.8; found: %C, 25.3;D %H, 4.7; %N, 11.7.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04824866 |
| Source dataset | uspto-grants-1989_04 |
| ORD ID | ord-3fe8fea3431d49788cec5587b5bf1f83 |
| Source note | uspto-grants-1989_04 |