HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 178504595, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium periodate | HCID 23667635 | — |
| Reactant | HCID 178503117 | HCID 178503117 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178504595 | HCID 178504595 | 65.7% |
Reaction Steps
To a suspension of 4-hydroxy-8-(4-methylthiophenyl)pyrazolo[1,5-a]-1,3,5-triazine (258 mg) and sodium metaperiodate (430 mg) in methanol (20 ml) is added water (0.5 ml), and the mixture is stirred at room temperature for 40 hours. The insoluble material is separated by filtration, washed with water and dried to give the title compound (180 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04824834 |
| Source dataset | uspto-grants-1989_04 |
| ORD ID | ord-ccc1779556774c6a87a3a1c26e3219e5 |
| Source note | uspto-grants-1989_04 |