HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 2-chloroacetoacetate → HCID 54697139, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 2-chloroacetoacetate | HCID 11858 | — |
| Reactant | Methyl Thioglycolate | HCID 16907 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 54697139 | HCID 54697139 | — |
Reaction Steps
Prepared by the method described in Example 1 from ethyl α-chloroacetoacetate (59 g, 0.35 moles), methyl thioglycolate (102 g, 0.70 moles) and sodium (19.7 g, 0.86 moles). The product is obtained from the crystalline precipitate by fractional recrystallization from isopropanol to give 2.8 g; mp 105°-107° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04824958 |
| Source dataset | uspto-grants-1989_04 |
| ORD ID | ord-33ad1e293a3e464d9e4c8db34ade3243 |
| Source note | uspto-grants-1989_04 |