HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 13770109, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 4-Cyclohexylmorpholine | HCID 22938 | — |
| Reactant | HCID 70416511 | HCID 70416511 | — |
| Product | HCID 13770109 | HCID 13770109 | — |
Reaction Steps
A solution of 10.9 g (0.033 mole) of ethyl 3-nitrobenzylidenebenzoylacetoacetate and 5.6 g (0.033 mole) of morpholinocyclohexane in 80 ml of ethanol is boiled under reflux for 4 hours. The solution is concentrated and the residue is triturated with ether, filtered off with suction and recrystallized from ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04769375 |
| Source dataset | uspto-grants-1988_09 |
| ORD ID | ord-322e4f1e9fcb482d876007b595fc1c6a |
| Source note | uspto-grants-1988_09 |