HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13813644, compound → HCID 14257077, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13813644 | HCID 13813644 | — |
| Solvent | Sulfuric Acid | HCID 1118 | — |
| Product | HCID 14257077 | HCID 14257077 | 118.1% |
Reaction Steps
Ten grams of α, α-diphenyl-5-pyrimidinemethanol were stirred in 50 ml of sulfuric acid for approximately 18 hours. The solution was poured onto ice and the resulting solids were recovered by filtration providing 11 g of the desired title product. Recrystallization from diethyl ether provided material with a melting point of 148°-150° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04769378 |
| Source dataset | uspto-grants-1988_09 |
| ORD ID | ord-dd7a51888b1e439690b50f286d6650ef |
| Source note | uspto-grants-1988_09 |