HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 17846762, compound → HCID 21293331, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 17846762 | HCID 17846762 | — |
| Reactant | HCID 21293332 | HCID 21293332 | — |
| Reactant | HCID 21293346 | HCID 21293346 | — |
| Product | HCID 21293331 | HCID 21293331 | — |
Reaction Steps
The procedure used was identical to that used in preparing 6-[2-(4-methoxyphenyl)ethenyl]-2-[2-(dimethylamino)ethyl]phthalazin-1(2H)-one (Example III above), except that 6-Bromo-2-[3-(dimethylamino)propyl]phthalazin-1(2H)-one was substituted for 6-Bromo-2-[2-(dimethyamino)ethyl]phthalazin-1(2H)-one. The weight of product obtained from 102 gm starting halide was 104 gm after recrystallization from 50 ml of methoxyethanol. It melted at 232°-234° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04769369 |
| Source dataset | uspto-grants-1988_09 |
| ORD ID | ord-53174ac763514d21a54b40c4374b1270 |
| Source note | uspto-grants-1988_09 |