1-Ethenyl-4-nitrobenzene → 4-Nitrobenzaldehyde

HRID 622168Notes

Reaction equation

HRID 622168 reaction equation
[N+:1]([C:4]1[CH:11]=[CH:10][C:7]([CH:8]=C)=[CH:6][CH:5]=1)([O-:3])=[O:2].[O:12]=[O+][O-]>CO>[N+:1]([C:4]1[CH:11]=[CH:10][C:7]([CH:8]=[O:12])=[CH:6][CH:5]=1)([O-:3])=[O:2]

Participants

4

Reactant 2

HCID 74811-Ethenyl-4-nitrobenzeneHCID 24823Ozone

Product 1

HCID 5414-Nitrobenzaldehyde

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

224 g of p-nitrostyrene are dissolved in 1 liter of methanol and reacted with ozone and subsequently hydrogenated analogously to the procedure indicated in Example 1. The absorption of hydrogen is 31.4 standard liters, corresponding to 93.4% of theory.

Workup

  1. customThe absorption of hydrogen

Sources & evidence

ORD record
ord-e8d9187cddb14d2c922702ff086e6208
Source dataset
uspto-grants-1988_09
Patent number
US04769464

Reaction notes

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