Ozone → HCID 13627713, compound

HRID 622170Notes

Reaction equation

HRID 622170 reaction equation
[CH2:1]([O:5][CH:6]([O:10][CH2:11][CH2:12][CH2:13][CH3:14])[CH2:7][CH:8]=C)[CH2:2][CH2:3][CH3:4].[O:15]=[O+][O-]>CO>[CH2:1]([O:5][CH:6]([O:10][CH2:11][CH2:12][CH2:13][CH3:14])[CH2:7][CH:8]=[O:15])[CH2:2][CH2:3][CH3:4]

Participants

4

Reactant 2

HCID 24823OzoneHCID 13627712HCID 13627712, compound

Product 1

HCID 13627713HCID 13627713, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Conditions

Temperature
35 °C

Procedure

300 g of 4,4-di-n-butoxybutene are dissolved in 1 liter of methanol and are reacted with ozone, and subsequently hydrogenated, analogously to the procedure indicated in Example 8. The hydrogenation is carried out in such a way that the content of peroxides in the hydrogenation solution does not exceed 0.02 mole/liter, and a pH value between 4 and 5 and a temperature of 35° C. are maintained. The consumption of hydrogen is 32.4 standard liters, corresponding to 96% of theory.

Workup

  1. customThe consumption of hydrogen

Sources & evidence

ORD record
ord-f91dcf8f70f74b1099636072a3def20d
Source dataset
uspto-grants-1988_09
Patent number
US04769464

Reaction notes

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