Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ozone | HCID 24823 | — |
| Reactant | HCID 13627712 | HCID 13627712 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 13627713 | HCID 13627713 | — |
Reaction Steps
300 g of 4,4-di-n-butoxybutene are dissolved in 1 liter of methanol and are reacted with ozone, and subsequently hydrogenated, analogously to the procedure indicated in Example 8. The hydrogenation is carried out in such a way that the content of peroxides in the hydrogenation solution does not exceed 0.02 mole/liter, and a pH value between 4 and 5 and a temperature of 35° C. are maintained. The consumption of hydrogen is 32.4 standard liters, corresponding to 96% of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04769464 |
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| Source dataset | uspto-grants-1988_09 |
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| ORD ID | ord-f91dcf8f70f74b1099636072a3def20d |
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| Source note | uspto-grants-1988_09 |
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