HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 622280Generated: October 25, 2026
Hydrochloric Acid → HCID 21292383, compound
https://huagongshe.com/reaction/622280
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 4-Amidinobenzamide Hydrochloride | HCID 2724293 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 53871664 | HCID 53871664 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21292383 | HCID 21292383 | — |
Reaction Steps
A solution of 480 mg of sodium in 17.5 ml of methanol is treated with 1.18 g of 3-methoxy-2-(5-hexenyl)acrolein and 1.62 g of 4-amidinobenzamide hydrochloride and the mixture is stirred at 50° C. overnight under nitrogen. After cooling the suspension is treated with 5.5 ml of 3N hydrochloric acid, filtered and the residue is washed with water and dried. The crude p-[5-(5-hexenyl)-2-pyrimidinyl]benzamide obtained is further processed without additional purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04770503 |
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| Source dataset | uspto-grants-1988_09 |
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| ORD ID | ord-a2b2e1c336c54b2ca4a417ae51b7bde7 |
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| Source note | uspto-grants-1988_09 |
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