Cyanuric chloride → 2,4-Dichloro-6-methoxy-3,5-triazine

Participants

Reaction Conditions

Reaction Steps

7 parts of sodium hydrogencarbonate was added to 50 parts of methanol. This mixture was cooled to 0° C. from outside. Then, 15 parts of cyanuric chloride was added to conduct a reaction for 60 minutes (First condensation). To the reaction mixture was added 100 parts of ice water, and the crystal precipitated was collected by filtration to obtain 2-methoxy-4,6-dichloro-1,3,5-triazine.

Provenance & Evidence