HRID622469

反应详情

EQUATION

反应方程式

HRID 622469 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

CONDITIONS

反应条件

温度
0 °C

PROCEDURE

实验过程

7 parts of sodium hydrogencarbonate was added to 50 parts of methanol. This mixture was cooled to 0° C. from outside. Then, 15 parts of cyanuric chloride was added to conduct a reaction for 60 minutes (First condensation). To the reaction mixture was added 100 parts of ice water, and the crystal precipitated was collected by filtration to obtain 2-methoxy-4,6-dichloro-1,3,5-triazine.

WORKUP

后处理

  1. customa reaction for 60 minutes
  2. custom(First condensation)
  3. customthe crystal precipitated
  4. filtrationwas collected by filtration