HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 20040999, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 14254900 | HCID 14254900 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20040999 | HCID 20040999 | — |
Reaction Steps
An ice water chilled solution of 5-methoxycarbonyl-1-[4-(4-methyl-1-piperazinyl)-2-butynyl]-2-pyrrolidinone (5.02 g) in sieve dried methanol (150 ml) was treated with anhydrous ammonia for fifteen minutes and was allowed to stand at ambient temperture overnight. The solution was concentrated to an amber oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04772601 |
| Source dataset | uspto-grants-1988_09 |
| ORD ID | ord-cafa44552cc84623b1dd1689acf2aca5 |
| Source note | uspto-grants-1988_09 |