HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 135617167, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 8-Amino-9-(2-thienylmethyl)guanine | HCID 135400908 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 135617167 | HCID 135617167 | — |
Reaction Steps
A mixture of 8-amino-9-[(2-thienyl)methyl]guanine (0.5 g; 1.88 mmol), DMF (10 ml), pyridine (5 ml), and acetic anhydride (5 ml) was stirred at room temperature for 36 hours. The mixture was diluted with ether (50 ml) and filtered to give analytically pure product, mp 243°-4° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04772606 |
| Source dataset | uspto-grants-1988_09 |
| ORD ID | ord-269cd4eedb054ca7af13eedc302ccae0 |
| Source note | uspto-grants-1988_09 |