Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 70417220 | HCID 70417220 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178482378 | HCID 178482378 | — |
Reaction Steps
The oxadiazole from Example 16 (3 g, 7.5 mmol) is dissolved in 25 ml of ethanol saturated with methylamine and the solution heated in a sealed tube at 50° C. for 16 hours. The mixture is concentrated to provide 3-[2-[(5-Dimethylaminomethyl-2-furanyl)methylthio]ethyl]-amino-5-methylamino-1,2,4-oxadiazole as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04772622 |
|---|
| Source dataset | uspto-grants-1988_09 |
|---|
| ORD ID | ord-88aedf588e7044ff8f01f9db60d72e11 |
|---|
| Source note | uspto-grants-1988_09 |
|---|
