HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine, hydrochloride → HCID 3554384, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine, hydrochloride | HCID 10473 | — |
| Reactant | HCID 70407058 | HCID 70407058 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 3554384 | HCID 3554384 | 72.2% |
Reaction Steps
97 weight-parts of dimethylamine hydrochloride are dissolved in 250 weight-parts of water, and 200 weight-parts of sodium 3-hydroxy-2-phenyl acrylic acid methyl ester are added. The mixture is stirred for 2 hours, and the organic phase is separated and distilled. 148 weight-parts of 3-dimethylamino-2-phenyl acrylic acid methyl ester are obtained, corresponding to a yield of 72.2% of the theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04772711 |
| Source dataset | uspto-grants-1988_09 |
| ORD ID | ord-42f29bb6a9ac4b9d87ac01e86138f738 |
| Source note | uspto-grants-1988_09 |