HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → Bis(1-methylethyl) B-phenylboronate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | Triisopropyl borate | HCID 21531 | — |
| Reactant | HCID 178506676 | HCID 178506676 | — |
| Product | Bis(1-methylethyl) B-phenylboronate | HCID 569210 | — |
Reaction Steps
Following the procedure of Example 9, phenyllithium (17 mL, 30.6 mmol) and triisopropoxyborane (5.6 g, 30 mmol) were reacted, and the reaction quenched with acetyl chloride (2.1 mL, 30 mmol) to yield after distillation 5.2 g (25.2 mmol, 84%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04772751 |
| Source dataset | uspto-grants-1988_09 |
| ORD ID | ord-9e6c2d94fac9448b966dfa51d02554bc |
| Source note | uspto-grants-1988_09 |