HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 14390490, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-chloropyridine-2-carbonyl Chloride | HCID 11095146 | — |
| Reactant | Ethyl 2-(3-aminopyridin-2-ylamino)acetate | HCID 14390203 | — |
| Product | HCID 14390490 | HCID 14390490 | — |
Reaction Steps
The crude 4-chloro picolinoyl chloride and triethylamine (5.55 g, 0.055 mole) were added dropwise simulaneously to the above stirred filtrate of N-(3-amino-2-pyridinyl)glycine ethyl ester at room temperature and allowed to stir overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04772600 |
| Source dataset | uspto-grants-1988_09 |
| ORD ID | ord-933ad28f3cb9484c9fa5ce048c49ee70 |
| Source note | uspto-grants-1988_09 |