HCID 21290604, compound → HCID 14010516, compound

Participants

Reaction Steps

30 g (0.1165 mol) of 2-(4-chlorophenyl)propane-1,3-diamine dihydrochloride are dissolved in the minimum quantity of water, NaOH is added until the pH is 11, the mixture is extracted with 4×100 ml of chloroform, the chloroform phase is washed with 50 ml of water, dried over MgSO4 and filtered, and the filtrate is evaporated to dryness to give 20.8 g (0.1127 mol) of 2-(4-chlorophenyl)propane-1,3-diamine.

Provenance & Evidence