1-Bromohexane → HCID 10704646, compound

Participants

Reaction Steps

5-Phenyltetrazole (29.2 g, 0.2 mole) was placed in 300 ml of ethanol and sodium methylate (11 g, 0.2 mole) added. On the addition of bromohexane (33 g, 0.2 mole), the solution cleared immediately. The mixture slowly became cloudy on four hours refluxing. Filtering followed by stripping gave 21.2 g of a yellow liquid.

Provenance & Evidence